Heating Under Reflux

In a reflux setup solvent vapors are trapped by the condenser and the concentration of reactants remains constant throughout the process. Best microwaveable heating pad for cramps.

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. Natural Life Shaped Heating Pad Sloth Best wearable heating pad for cramps. Reflux is shared under a CC BY-NC-ND. Introducing the worlds first weighted heating pad Sharper Image Calming Heat by Calming Comfort.

The secret is the heat absorbing clay beads that retain and evenly distribute the soothing heat. A reflux apparatus allows for facile heating of a solution but without the loss of solvent that would result from heating in an open vessel. Calming Heat provides the soothing heat therapy of a heating pad with the added benefit of weight- 4 pounds.

Start water flowing through jacket of the reflux condenser and apply air pressure to the stirring motor to produce vigorous agitation. Add 1 liter of solvent and clamp top in position. Turn on heating jacket with transformer set at a predetermined voltage to bring the temperature of the contents to 50 degC within 20-25 minutes.

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